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Beilstein J. Org. Chem. 2017, 13, 106–110, doi:10.3762/bjoc.13.13
Graphical Abstract
Scheme 1: Automated synthesis of 4a.
Figure 1: Full picture of ChemKonzert, showing two reaction vessels (RF1 and RF2), a centrifugal separator (S...
Beilstein J. Org. Chem. 2013, 9, 2336–2343, doi:10.3762/bjoc.9.268
Figure 1: Sterically crowded, and neutral chelating diimine ligands.
Scheme 1: One-step synthesis of the ligand 3b, and a plausible decomposition pathway for 3b to naphthylamine (...
Figure 2: Micro-flow synthesis of the ligands 3b and 3c.
Figure 3: ORTEP drawing of 3b. Thermal ellipsoids are set at 35% probability level. Hydrogen atoms are omitte...
Scheme 2: Synthesis of the ligand 3c through the coupling of 4 and 9.
Figure 4: ORTEP drawing of 3c. Thermal ellipsoids are set at 35% probability level. Hydrogen atoms are omitte...
Scheme 3: Complexation of the ligands 3b and 3c with NiBr2(dme).
Figure 5: ORTEP drawing of 12. Thermal ellipsoids are set at 35% probability level. Hydrogen atoms and cocrys...